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453, 643 Behera, S

weighing 4.2 g (14mmol) of Fmoc-Gly-OH, 2.2 g (16.8mmol) of HOBt and 0.2 g (1.4mmol) of DMAP, dissolving with DMF, adding 3.0ml of DIC (20mmol) in an ice-water bath at 0 , activating for 5 minutes, adding the mixture into a reaction column, reacting for 2 hours, adding 35ml of acetic anhydride and 30ml of pyridine, mixing and sealing for 24 hours, washing three times with DCM, draining the Resin after methanol contraction to obtain 23.2 g of 1- (2-hydroxyethyl) imidazole tetrafluoroboric acid-Merrifield Resin, and detecting the substitution degree to be 0.26 mmol/g